5HFZ
Mmi1 YTH domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-12-18 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97920 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 57.984, 57.984, 370.834 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.761 - 1.960 |
R-factor | 0.2075 |
Rwork | 0.205 |
R-free | 0.25100 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.009 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.000 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.531 | |
Number of reflections | 46677 | |
<I/σ(I)> | 24.8 | 2.9 |
Completeness [%] | 86.3 | 58 |
Redundancy | 3.3 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 295 | 0.1 M lithium chloride, 0.1 M Hepes (pH 7.3), 25% PEG6000. |