5HCE
Ternary complex of human Complement C5 with Ornithodoros moubata OmCI and Rhipicephalus appendiculatus RaCI1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-16 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97949 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 105.260, 140.725, 210.367 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 74.403 - 3.120 |
R-factor | 0.268 |
Rwork | 0.267 |
R-free | 0.28080 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3cu7 2cm4 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.746 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 94.100 | 3.310 |
High resolution limit [Å] | 3.120 | 3.120 |
Rmerge | 0.115 | 0.953 |
Number of reflections | 56166 | |
<I/σ(I)> | 8.2 | 1.4 |
Completeness [%] | 99.7 | 99.7 |
Redundancy | 4.4 | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9 | 294 | 10% PEG 6K, 0.1 M Bicine pH 9.0 |