5H9H
holo acyl carrier protein (holo-ACP) from Helicobacter pylori
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-X |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-12-01 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 |
Unit cell lengths | 50.344, 50.344, 73.300 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.600 - 2.500 |
R-factor | 0.218 |
Rwork | 0.216 |
R-free | 0.25200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1t8k |
RMSD bond length | 0.013 |
RMSD bond angle | 1.484 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.270 | |
Number of reflections | 6736 | |
<I/σ(I)> | 2.3 | 2.3 |
Completeness [%] | 98.5 | 97.8 |
Redundancy | 3 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 4 | 277 | 0.5 M Ammonium Sulfate, 0.1 M tri-Sodium Citrate dihydrate, 1 M Lithium Sulfate monohydrate |