5H6J
DNA targeting ADP-ribosyltransferase Pierisin-1 in complex with beta-NAD+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2008-12-20 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 93.328, 93.328, 120.660 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.738 - 1.900 |
R-factor | 0.26408 |
Rwork | 0.263 |
R-free | 0.27991 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.028 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 43.520 |
High resolution limit [Å] | 1.900 |
Number of reflections | 42294 |
<I/σ(I)> | 20.4 |
Completeness [%] | 98.9 |
Redundancy | 13.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M NaF, 6-10% (w/v) PEG 3350 |