Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 12.3.1 |
| Synchrotron site | ALS |
| Beamline | 12.3.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-03-11 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97888 |
| Spacegroup name | P 31 |
| Unit cell lengths | 48.648, 48.648, 118.090 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 24.324 - 2.122 |
| R-factor | 0.2295 |
| Rwork | 0.223 |
| R-free | 0.25900 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.098 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.7.3_928) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 2.120 |
| Number of reflections | 17702 |
| <I/σ(I)> | 18 |
| Completeness [%] | 98.0 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298 | 100mM Tris pH 7.0, 20% PEG 3350 MME |
