5H4C
Crystal structure of Cbln4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-10-31 |
Detector | RAYONIX MX-325 |
Wavelength(s) | 0.9199 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 91.198, 91.198, 148.693 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.300 |
R-factor | 0.17829 |
Rwork | 0.176 |
R-free | 0.21359 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.132 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.300 |
Number of reflections | 28464 |
<I/σ(I)> | 15.8 |
Completeness [%] | 99.8 |
Redundancy | 9.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 4% Tacsimate, pH 7.0, 12% PEG 3350 |