5H4B
Crystal structure of Cbln4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NFPSS BEAMLINE BL19U1 |
Synchrotron site | NFPSS |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-03-28 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9788 |
Spacegroup name | P 43 3 2 |
Unit cell lengths | 132.357, 132.357, 132.357 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.800 |
R-factor | 0.2085 |
Rwork | 0.207 |
R-free | 0.23282 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.299 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.800 |
Number of reflections | 10335 |
<I/σ(I)> | 23.5 |
Completeness [%] | 99.9 |
Redundancy | 9.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.2 | 298 | 2.5 M NaCl, Na/K phosphate, pH6.2 |