5H48
Crystal structure of Cbln1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-10-31 |
Detector | RAYONIX MX-325 |
Wavelength(s) | 0.9199 |
Spacegroup name | P 6 |
Unit cell lengths | 82.981, 82.981, 50.543 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 71.860 - 2.200 |
R-factor | 0.16476 |
Rwork | 0.163 |
R-free | 0.20297 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4nn0 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.567 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 71.860 |
High resolution limit [Å] | 2.200 |
Number of reflections | 9670 |
<I/σ(I)> | 13.1 |
Completeness [%] | 94.7 |
Redundancy | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.2 M Sodium tartrate dibasic dihydrate, 20% PEG3350, pH 7.3 |