5H1E
Interaction between vitamin D receptor and coactivator peptide SRC2-3
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-5A |
| Synchrotron site | Photon Factory |
| Beamline | BL-5A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-12-20 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.00000 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 155.770, 42.880, 42.210 |
| Unit cell angles | 90.00, 95.83, 90.00 |
Refinement procedure
| Resolution | 41.990 - 2.600 |
| R-factor | 0.23966 |
| Rwork | 0.239 |
| R-free | 0.24834 |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.542 |
| Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 41.990 |
| High resolution limit [Å] | 2.600 |
| Number of reflections | 6752 |
| <I/σ(I)> | 73.3 |
| Completeness [%] | 78.0 |
| Redundancy | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | MOP-Na, Na-Formate, PEG 4000, Ethleneglycol |
