5H10
TRAF1-TANk complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2016-06-01 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 77.210, 79.034, 113.380 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.890 - 3.205 |
R-factor | 0.2235 |
Rwork | 0.218 |
R-free | 0.26980 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5e1t |
RMSD bond length | 0.002 |
RMSD bond angle | 0.517 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.250 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.065 | 0.172 |
Number of reflections | 11811 | |
<I/σ(I)> | 42.34 | |
Completeness [%] | 99.5 | |
Redundancy | 10.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 1.38M Ammonium sulfate, 0.1M CHES pH 9.3, 200mM NaCl |