5H07
TNIP2-Ub complex, C2 form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13C1 |
Synchrotron site | NSRRC |
Beamline | BL13C1 |
Temperature [K] | 113 |
Detector technology | CCD |
Collection date | 2015-07-12 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.975 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 98.765, 80.972, 65.352 |
Unit cell angles | 90.00, 114.28, 90.00 |
Refinement procedure
Resolution | 19.858 - 2.586 |
R-factor | 0.2177 |
Rwork | 0.211 |
R-free | 0.27340 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.517 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.586 |
Number of reflections | 12803 |
<I/σ(I)> | 13.4 |
Completeness [%] | 99.2 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | ammonium acetate, PEG3350, Tris-HCl |