5GZD

Galectin-8 N-terminal domain carbohydrate recognition domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-06-19
Detector	DECTRIS PILATUS 12M
Wavelength(s)	0.9785
Spacegroup name	C 1 2 1
Unit cell lengths	60.527, 40.052, 56.179
Unit cell angles	90.00, 108.93, 90.00

Refinement procedure

Resolution	18.995 - 1.190
R-factor	0.2006
Rwork	0.200
R-free	0.21240
Refinement software	PHENIX (1.10.1_2155)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.000
High resolution limit [Å]	1.190
Number of reflections	40642
<I/σ(I)>	17.5
Completeness [%]	99.3
Redundancy	6.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG 2000MME