5GW0
Crystal structure of SNX16 PX-Coiled coil
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-04-18 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9791 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 70.380, 196.780, 72.960 |
Unit cell angles | 90.00, 111.75, 90.00 |
Refinement procedure
Resolution | 19.991 - 3.300 |
R-factor | 0.239 |
Rwork | 0.236 |
R-free | 0.28800 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.381 |
Data reduction software | Aimless |
Data scaling software | Aimless (0.5.12) |
Phasing software | MR-Rosetta |
Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 56.770 | 56.770 | 3.500 |
High resolution limit [Å] | 3.300 | 9.900 | 3.300 |
Rmerge | 0.087 | 0.056 | 0.633 |
Rmeas | 0.102 | 0.066 | 0.741 |
Rpim | 0.052 | 0.034 | 0.383 |
Total number of observations | 98589 | 3117 | 16305 |
Number of reflections | 27200 | ||
<I/σ(I)> | 10.6 | 33 | 2.1 |
Completeness [%] | 98.3 | 83.4 | 99.5 |
Redundancy | 3.6 | 3.6 | 3.6 |
CC(1/2) | 0.996 | 0.993 | 0.647 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 277 | 31mM Citric, 69mM Bis-tris Propanol, 18% PEG 5000, 70mM NaF, 2mM TCEP |