5GVV
Crystal structure of the glycosyltransferase GlyE in Streptococcus pneumoniae TIGR4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-04-15 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97915 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 75.170, 88.210, 128.360 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.810 - 1.950 |
R-factor | 0.2066 |
Rwork | 0.204 |
R-free | 0.25730 |
Structure solution method | SAD |
RMSD bond length | 0.005 |
RMSD bond angle | 0.942 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.810 | 2.060 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.133 | 0.394 |
Number of reflections | 61392 | |
<I/σ(I)> | 7.3 | 3 |
Completeness [%] | 97.7 | 93.9 |
Redundancy | 4.9 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 289 | 0.2 M MgCl2, 0.1 M HEPES, pH 7.5, 25% PEG 3350 |