5GVJ
Structure of FabK (M276A) mutant from Thermotoga maritima
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-05-12 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 84.096, 115.129, 67.913 |
Unit cell angles | 90.00, 106.59, 90.00 |
Refinement procedure
Resolution | 34.649 - 1.900 |
R-factor | 0.1817 |
Rwork | 0.181 |
R-free | 0.20720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5gvh |
RMSD bond length | 0.007 |
RMSD bond angle | 0.829 |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 48755 | |
<I/σ(I)> | 39.5 | |
Completeness [%] | 96.3 | |
Redundancy | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 295 | 20 mM Tris-HCl (pH 8.0), 150 mM NaCl, 1 mM DTT 1 mM FMN |