5GVA
WD40 domain of human AND-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-03-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.91769 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.895, 79.895, 163.744 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.148 - 1.851 |
R-factor | 0.1709 |
Rwork | 0.170 |
R-free | 0.18840 |
Structure solution method | SIRAS |
RMSD bond length | 0.008 |
RMSD bond angle | 1.075 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELXDE |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.880 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 45822 | |
<I/σ(I)> | 30.48 | |
Completeness [%] | 99.5 | 94.7 |
Redundancy | 7.7 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 1.8M Ammonium citrate tribasic pH7.5 |