5GT1
crystal structure of cbpa from L. salivarius REN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17B1 |
Synchrotron site | SSRF |
Beamline | BL17B1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-24 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.1000 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 95.724, 95.724, 39.318 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.850 |
R-factor | 0.17282 |
Rwork | 0.172 |
R-free | 0.19687 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b0p |
RMSD bond length | 0.009 |
RMSD bond angle | 1.193 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | BALBES |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.880 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 16222 | |
<I/σ(I)> | 29.8 | |
Completeness [%] | 91.9 | |
Redundancy | 8.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289 | 1.0 M (NH4)2HPO4, 0.1 M Acetate |