5GPK
Crystal structure of Ccp1 mutant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-05-01 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.97923 |
Spacegroup name | P 41 2 2 |
Unit cell lengths | 86.814, 86.814, 158.776 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.824 - 2.103 |
R-factor | 0.1786 |
Rwork | 0.176 |
R-free | 0.22520 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.033 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 36042 | |
<I/σ(I)> | 23.86 | |
Completeness [%] | 99.7 | |
Redundancy | 13.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 289 | 100mM C3H2Na2O4, 200mM NH4NO3, 18% PEG 3350, 15% EG |