5GPD
Crystal structure of the binding domain of SREBP from fission yeast
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-04-30 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 96.903, 96.903, 151.595 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.973 - 3.501 |
R-factor | 0.2661 |
Rwork | 0.265 |
R-free | 0.27850 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.090 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.630 |
High resolution limit [Å] | 3.500 | 3.500 |
Rmerge | 0.060 | 0.497 |
Number of reflections | 10643 | |
<I/σ(I)> | 18.5 | 2.9 |
Completeness [%] | 98.1 | 99.8 |
Redundancy | 3.2 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M BTP (pH 7.0), 1.5M NaNO3 |