5GPC
Structural analysis of fatty acid degradation regulator FadR from Bacillus halodurans
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-03-11 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.97933 |
Spacegroup name | P 1 |
Unit cell lengths | 46.500, 76.935, 87.022 |
Unit cell angles | 103.83, 105.48, 89.64 |
Refinement procedure
Resolution | 19.904 - 2.800 |
R-factor | 0.2081 |
Rwork | 0.205 |
R-free | 0.26560 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5gp9 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.773 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.850 |
High resolution limit [Å] | 2.800 | 7.590 | 2.800 |
Rmerge | 0.101 | 0.045 | 0.608 |
Number of reflections | 26864 | ||
<I/σ(I)> | 9 | ||
Completeness [%] | 96.3 | 94.6 | 96.2 |
Redundancy | 2.1 | 1.9 | 2 |
CC(1/2) | 0.990 | 0.603 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 296 | HEPES, PEG 8000, ethanol |