5GOR
Crystal structure of alkaline invertase InvA from Anabaena sp. PCC 7120
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-09-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97930 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 96.171, 179.282, 96.362 |
Unit cell angles | 90.00, 105.92, 90.00 |
Refinement procedure
Resolution | 30.497 - 2.673 |
R-factor | 0.194 |
Rwork | 0.192 |
R-free | 0.23490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5goo |
RMSD bond length | 0.010 |
RMSD bond angle | 0.976 |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.770 |
High resolution limit [Å] | 2.670 | 2.670 |
Number of reflections | 84349 | |
<I/σ(I)> | 10.8 | 3.1 |
Completeness [%] | 95.4 | 97 |
Redundancy | 2.9 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9 | 287 | 27% PEG 6k, 0.1 M Becine |