5GNY
The structure of WT Bgl6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-11-29 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 68.358, 159.696, 197.360 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.973 - 2.105 |
R-factor | 0.1986 |
Rwork | 0.197 |
R-free | 0.23640 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1oin |
RMSD bond length | 0.003 |
RMSD bond angle | 0.819 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.156 | 0.922 |
Number of reflections | 125484 | |
<I/σ(I)> | 10.1 | 1.74 |
Completeness [%] | 99.2 | 97.8 |
Redundancy | 4.7 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.8 | 298 | 25% PEG 8K, 70 mM NaCl, 100 mM Tris-HCl pH 7.8 |