5GNC
Crystal structure of Phytophthora. sojae PSR2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-11-21 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97915 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 86.320, 49.720, 94.450 |
Unit cell angles | 90.00, 110.88, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.800 |
R-factor | 0.2117 |
Rwork | 0.208 |
R-free | 0.26640 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.128 |
Data scaling software | HKL-2000 |
Phasing software | AutoSol |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.800 |
Number of reflections | 18820 |
<I/σ(I)> | 2.8 |
Completeness [%] | 98.8 |
Redundancy | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20% PEG 3350, 0.2M NH4COOH |