5GMI
Crystal Structure of GRASP55 GRASP domain in complex with JAM-C C-terminus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-02-25 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.075 |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 132.492, 132.492, 220.706 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 71.420 - 2.710 |
R-factor | 0.259 |
Rwork | 0.256 |
R-free | 0.29100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3rle |
RMSD bond length | 0.005 |
RMSD bond angle | 1.066 |
Data reduction software | HKL-2000 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 71.420 | 2.810 |
High resolution limit [Å] | 2.710 | 2.711 |
Rmerge | 0.137 | 0.667 |
Number of reflections | 27006 | |
<I/σ(I)> | 7.1 | 2.38 |
Completeness [%] | 99.9 | 100 |
Redundancy | 6.1 | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 291 | SODIUM FORMATE, SODIUM ACETATE |