5GKE
Structure of EndoMS-dsDNA1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-07-16 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0000 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 92.360, 92.360, 404.290 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.790 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 40879 | |
<I/σ(I)> | 96.2 | 9.1 |
Completeness [%] | 98.8 | 94.6 |
Redundancy | 3.9 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | CALCIUM ACETATE, SODIUM CACODYLATE, PEG8000, GLYCEROL |