5GIY
HSA-Palmitic acid-[RuCl5(ind)]2-
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-10-20 |
Detector | Nonius Kappa CCD |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 185.845, 38.710, 96.070 |
Unit cell angles | 90.00, 105.12, 90.00 |
Refinement procedure
Resolution | 46.429 - 2.543 |
R-factor | 0.2273 |
Rwork | 0.224 |
R-free | 0.27860 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bj5 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.523 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 47.000 |
High resolution limit [Å] | 2.500 |
Number of reflections | 22025 |
<I/σ(I)> | 4 |
Completeness [%] | 97.0 |
Redundancy | 4.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 7 | 293 | 28 PEG3350, 6% glycerol, 4% DMSO. |