5G4U
Association of three two-k-turn units based on Kt-7 3bU,3nU, forming a triangular-shaped structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-20 |
Detector | DECTRIS PIXEL |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 261.260, 69.220, 85.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 51.870 - 2.650 |
R-factor | 0.23 |
Rwork | 0.229 |
R-free | 0.25800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bw0 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.129 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.250 | 2.720 |
High resolution limit [Å] | 2.650 | 2.650 |
Rmerge | 0.100 | 1.500 |
Number of reflections | 45710 | |
<I/σ(I)> | 12.6 | 1 |
Completeness [%] | 99.4 | 99.6 |
Redundancy | 5.3 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 1.6 M TRI-SODIUM CITRATE DIHYDRATE (PH 6.5) |