5G4D
Crystal structure of the Cas2 in T.onnurineus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 287 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 29.515, 32.802, 83.161 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.753 - 1.701 |
R-factor | 0.2178 |
Rwork | 0.215 |
R-free | 0.24070 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 0.814 |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.700 |
Rmerge | 0.050 |
Number of reflections | 9301 |
Completeness [%] | 99.1 |
Redundancy | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | pH 7.0 |