5G42
Ligand complex of RORg LBD
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 62.060, 62.060, 159.120 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 43.880 - 1.720 |
| R-factor | 0.1863 |
| Rwork | 0.185 |
| R-free | 0.21240 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 0.920 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | BUSTER |
| Refinement software | BUSTER (2.11.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 51.300 | 1.780 |
| High resolution limit [Å] | 1.720 | 1.720 |
| Rmerge | 0.090 | |
| Number of reflections | 33994 | |
| <I/σ(I)> | 19 | 1.8 |
| Completeness [%] | 99.9 | 99.6 |
| Redundancy | 12.5 | 13.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
