5G42
Ligand complex of RORg LBD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 62.060, 62.060, 159.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.880 - 1.720 |
R-factor | 0.1863 |
Rwork | 0.185 |
R-free | 0.21240 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 0.920 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | BUSTER |
Refinement software | BUSTER (2.11.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.300 | 1.780 |
High resolution limit [Å] | 1.720 | 1.720 |
Rmerge | 0.090 | |
Number of reflections | 33994 | |
<I/σ(I)> | 19 | 1.8 |
Completeness [%] | 99.9 | 99.6 |
Redundancy | 12.5 | 13.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |