5G28
The crystal structure of light-driven chloride pump ClR at pH 6.0.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2015-07-27 |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 102.756, 49.402, 69.327 |
Unit cell angles | 90.00, 109.85, 90.00 |
Refinement procedure
Resolution | 65.210 - 1.570 |
R-factor | 0.15594 |
Rwork | 0.154 |
R-free | 0.19378 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3x3b |
RMSD bond length | 0.026 |
RMSD bond angle | 1.904 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.210 | 1.590 |
High resolution limit [Å] | 1.570 | 1.570 |
Rmerge | 0.110 | 0.660 |
Number of reflections | 45878 | |
<I/σ(I)> | 30.81 | 2.58 |
Completeness [%] | 97.2 | 90.7 |
Redundancy | 4.4 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | pH 6.0 |