5G1M
Crystal structure of NagZ from Pseudomonas aeruginosa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-03-27 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.971, 75.289, 76.389 |
Unit cell angles | 90.00, 110.10, 90.00 |
Refinement procedure
Resolution | 46.959 - 1.800 |
R-factor | 0.1979 |
Rwork | 0.196 |
R-free | 0.24060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2oxn |
RMSD bond length | 0.008 |
RMSD bond angle | 1.064 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.960 | 1.840 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.110 | 0.940 |
Number of reflections | 63078 | |
<I/σ(I)> | 9.5 | 1.7 |
Completeness [%] | 99.9 | 100 |
Redundancy | 5.8 | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 30% PEG 8000 100 MM SODIUM CACODYLATE PH 6.0 200 MM SODIUM ACETATE PH 6.0 |