5FZW
High resolution solution NMR structure of the spider venom peptide U3- scytotoxin-Sth1h
Spectrometer
Experimental method: SOLUTION NMR
Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
1 | Bruker | AVANCE | 600 | |
2 | Bruker | AVANCE | 600 |
Experiment
experiment id | conditions id | solution id | Experiment type |
1 | 1 | 1 | 13C ARO HSQC NOESY |
10 | 1 | 1 | 1H TOCSY |
11 | 1 | 1 | HCCH TOCSY |
12 | 1 | 1 | HNCACB |
13 | 1 | 1 | HNCACO |
14 | 1 | 1 | HNCO |
15 | 1 | 1 | HNCOCACB |
16 | 2 | 2 | 15N HSQC (15N SAMPLE) |
17 | 2 | 2 | 1H TOCSY (15N SAMPLE) |
18 | 2 | 2 | NOESY 120MS (15N SAMPLE) |
19 | 2 | 2 | NOESY 200MS (15N SAMPLE) |
2 | 1 | 1 | 13C AROMATIC HSQC |
3 | 1 | 1 | 13C CT-HSQC |
4 | 1 | 1 | 13C HSQC |
5 | 1 | 1 | 13C HSQC NOESY |
6 | 1 | 1 | 15N HMQC |
7 | 1 | 1 | 15N HMQC 2 |
8 | 1 | 1 | 15N HSQC NOESY |
9 | 1 | 1 | 1H NOESY (120MS) |
NMR Sample
conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
1 | 6.5 | 1.0 | 298 |
2 | 6.5 | 1.0 | 298 |
Conformers
Conformers Calculated Total Number | 100 |
Conformers Submitted Total Number | 20 |