5FZV
High resolution solution NMR structure of the spider venom peptide U3- scytotoxin-Sth1a
Spectrometer
Experimental method: SOLUTION NMR
Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
1 | Bruker | AVANCE | 600 | |
2 | Bruker | AVANCE | 600 |
Experiment
experiment id | conditions id | solution id | Experiment type |
1 | 1 | 1 | 13C ARO NOESY 160MS |
10 | 1 | 1 | HNCACO |
11 | 1 | 1 | HNCO |
12 | 1 | 1 | HNCOCACB |
13 | 2 | 2 | 15N HMQC |
14 | 2 | 2 | 15N HSQC-TOCSY |
15 | 2 | 2 | 1H NOESY (200MS) |
16 | 2 | 2 | 1H TOCSY |
2 | 1 | 1 | 13C AROMATIC HSQC |
3 | 1 | 1 | 13C CT-HSQC |
4 | 1 | 1 | 13C HSQC |
5 | 1 | 1 | 13C NOESY 160MS |
6 | 1 | 1 | 15N HMQC2 |
7 | 1 | 1 | 15N NOESY 160MS |
8 | 1 | 1 | HCCH TOCSY |
9 | 1 | 1 | HNCACB |
NMR Sample
conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
1 | 6.5 | 1.0 | 298 |
2 | 6.5 | 1.0 | 298 |
Conformers
Conformers Calculated Total Number | 100 |
Conformers Submitted Total Number | 20 |