5FWZ
Fasciola hepatica calcium binding protein FhCaBP2: Structure of the dynein light chain-like domain. P41212 mercury derivative.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-30 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 59.880, 59.880, 81.320 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 22.830 - 2.300 |
R-factor | 0.1965 |
Rwork | 0.191 |
R-free | 0.24051 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.012 |
RMSD bond angle | 1.469 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | autoSHARP |
Refinement software | REFMAC (5.8.0131) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 23.000 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.120 | 0.470 |
Number of reflections | 7026 | |
<I/σ(I)> | 12 | 4.5 |
Completeness [%] | 99.9 | 100 |
Redundancy | 9.6 | 9.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 10 MM TRIS-HCL PH 8.5, 50 MM SODIUM CHLORIDE 20 % (W/V) PEG 3350, 0.2 M SODIUM TARTRATE |