5FWU
Wnt modulator Kremen crystal form II at 2.8A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-15 |
Detector | DECTRIS PILATUS |
Spacegroup name | P 43 |
Unit cell lengths | 65.780, 65.780, 75.014 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 65.780 - 2.800 |
R-factor | 0.22003 |
Rwork | 0.216 |
R-free | 0.30707 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.019 |
RMSD bond angle | 1.952 |
Data reduction software | XDS |
Data scaling software | Aimless |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 75.000 |
High resolution limit [Å] | 2.800 |
Rmerge | 0.060 |
Number of reflections | 7964 |
<I/σ(I)> | 14.9 |
Completeness [%] | 99.8 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.6 | 0.1 M NA3CITRATE, 1.0 M MGSO4, FINAL PH 5.6 |