5FS0
crystal structure of the phenol-responsive sensory domain of the transcription activator PoxR with 2,4-dichlorophenol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 287 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.693, 70.872, 104.852 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.346 - 2.400 |
R-factor | 0.1854 |
Rwork | 0.181 |
R-free | 0.25800 |
Structure solution method | MIR |
Starting model (for MR) | NONE |
RMSD bond length | 0.007 |
RMSD bond angle | 0.990 |
Refinement software | PHENIX ((PHENIX.REFINE: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.820 |
High resolution limit [Å] | 1.790 | 1.790 |
Rmerge | 0.080 | |
Number of reflections | 33443 | |
<I/σ(I)> | 49.41 | 1 |
Completeness [%] | 99.2 | 89.6 |
Redundancy | 13.7 | 10.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |