5FPK
MONOMERIC RADA IN COMPLEX WITH FATA TETRAPEPTIDE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-03-08 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.302, 60.578, 87.447 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.723 - 1.343 |
R-factor | 0.1251 |
Rwork | 0.123 |
R-free | 0.16370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4b3b |
RMSD bond length | 0.009 |
RMSD bond angle | 1.033 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | AMoRE |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.800 | 1.420 |
High resolution limit [Å] | 1.340 | 1.340 |
Rmerge | 0.070 | 0.610 |
Number of reflections | 47749 | |
<I/σ(I)> | 22.41 | 2.98 |
Completeness [%] | 98.3 | 92.3 |
Redundancy | 6.98 | 6.24 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.2 | 8% PEG-1000, 100 MM NAK PHOSPHATE, PH 6.2 |