5FMI
Human Bak Q77L
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 58.024, 54.528, 58.716 |
Unit cell angles | 90.00, 115.50, 90.00 |
Refinement procedure
Resolution | 26.187 - 1.491 |
R-factor | 0.1868 |
Rwork | 0.185 |
R-free | 0.21150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ims |
RMSD bond length | 0.005 |
RMSD bond angle | 0.705 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.190 | 1.540 |
High resolution limit [Å] | 1.490 | 1.490 |
Rmerge | 0.030 | 0.160 |
Number of reflections | 26752 | |
<I/σ(I)> | 26.6 | 7.5 |
Completeness [%] | 98.9 | 99.6 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.5 | 10% PEG 3350, 0.1M SODIUM ACETATE PH 4.5, 20 MM ZINC ACETATE |