5FK1
SAM-I riboswitch bearing the H. marismortui Kt-7 variant 3bn is UG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 173 |
Detector technology | PIXEL |
Collection date | 2013-09-24 |
Detector | DECTRIS PIXEL |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 62.580, 62.580, 154.730 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 58.015 - 2.500 |
R-factor | 0.2414 |
Rwork | 0.238 |
R-free | 0.28900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5fjc |
RMSD bond length | 0.002 |
RMSD bond angle | 0.636 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 77.360 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.060 | 1.500 |
Number of reflections | 11293 | |
<I/σ(I)> | 11.3 | 1.1 |
Completeness [%] | 99.8 | 99.7 |
Redundancy | 5.6 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 40 MM NA-CACODYLATE (PH 7.0), 80 MM KCL, 50 MM BACL2, 12 MM SPERMINE-HCL, 10% (V/V) MPD. |