5FK0
Yeast delta-COP-I mu-homology domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2009-04-17 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 86.900, 148.630, 222.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.410 - 3.000 |
R-factor | 0.19696 |
Rwork | 0.195 |
R-free | 0.23330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5fjw |
RMSD bond length | 0.010 |
RMSD bond angle | 1.376 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.000 | 3.160 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.100 | 0.870 |
Number of reflections | 55431 | |
<I/σ(I)> | 8.5 | 1.7 |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 3.6 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | pH 7.0 |