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5FJW

Yeast delta-COP-I mu-homology domain complexed with Dsl1 WxWx(MSE) peptide

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I03
Synchrotron siteDiamond
BeamlineI03
Temperature [K]100
Detector technologyPIXEL
Collection date2011-06-02
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.97631, 0.97949, 0.97961
Spacegroup nameP 1
Unit cell lengths68.406, 79.298, 163.346
Unit cell angles79.71, 87.50, 83.60
Refinement procedure
Resolution160.670 - 2.800
R-factor0.17385
Rwork0.170
R-free0.23949
Structure solution methodMAD
Starting model (for MR)NONE
RMSD bond length0.012
RMSD bond angle1.683
Data reduction softwareMOSFLM
Data scaling softwareAimless
Phasing softwareautoSHARP
Refinement softwareREFMAC (5.8.0135)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]77.6002.850
High resolution limit [Å]2.8002.800
Rmerge0.1501.210
Number of reflections80910
<I/σ(I)>12.91.1
Completeness [%]97.897.4
Redundancy77.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
170.1MHEPES-NA PH 7.0, 0.15M(NH4)2SO4, 21%W/V PEG2250

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