5FHI
Crystallographic structure of PsoE without Co
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-30 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 1.10 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 145.413, 145.413, 51.266 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.598 - 2.410 |
R-factor | 0.1908 |
Rwork | 0.185 |
R-free | 0.24560 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.448 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | AutoSol |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.410 |
Number of reflections | 12786 |
<I/σ(I)> | 30.54 |
Completeness [%] | 99.8 |
Redundancy | 19.45 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEGmme 5000 |