Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-07-12 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 0.9650 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 54.660, 44.370, 92.510 |
| Unit cell angles | 90.00, 104.09, 90.00 |
Refinement procedure
| Resolution | 41.439 - 2.600 |
| R-factor | 0.2166 |
| Rwork | 0.215 |
| R-free | 0.25000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1yks |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.542 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | MOLREP |
| Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.700 |
| High resolution limit [Å] | 2.600 | 2.600 |
| Rmerge | 0.285 | |
| Number of reflections | 12626 | |
| Completeness [%] | 99.0 | 93 |
| Redundancy | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.5 | 277 | PEG 10000, HEPES |
