5FFI
[2Fe:2S] ferredoxin FeSII from Azotobacter vinelandii
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-02 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.0003 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 133.271, 134.480, 36.769 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 94.660 - 2.170 |
R-factor | 0.1967 |
Rwork | 0.195 |
R-free | 0.22930 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.120 |
Data reduction software | autoPROC |
Data scaling software | Aimless ((version 0.5.12)) |
Phasing software | autoSHARP |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 94.660 | 2.177 |
High resolution limit [Å] | 2.169 | 2.169 |
Rmerge | 0.149 | 1.380 |
Number of reflections | 36128 | |
<I/σ(I)> | 13.2 | 2.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.2 | 12.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 1 M of tri-sodium citrate 0.01 M sodium tetraborate (Na2B4O7) |