5FEY
TRIM32 RING
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-06-15 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.28254 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 54.536, 54.536, 99.120 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.781 - 2.230 |
| R-factor | 0.249 |
| Rwork | 0.248 |
| R-free | 0.27260 |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.486 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | AutoSol |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.781 | |
| High resolution limit [Å] | 2.230 | |
| Rmerge | 0.140 | 0.962 |
| Number of reflections | 7770 | |
| <I/σ(I)> | 13.28 | |
| Completeness [%] | 99.6 | |
| Redundancy | 20 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 291 | 0.1 M MES pH 6.0 and 5 % PEG 600 |
