5FD1

CRYSTAL STRUCTURES OF OXIDIZED AND REDUCED AZOTOBACTER VINELANDII FERREDOXIN AT PH 8 AND PH 6

Replaces:  4FD1Replaces:  1FD1Replaces:  2FD1Replaces:  3FD1

Experimental procedure

Spacegroup name	P 41 21 2
Unit cell lengths	55.200, 55.200, 95.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 1.900
R-factor	0.215
Rwork	0.215
RMSD bond length	0.014
RMSD bond angle	3.310
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000 *
High resolution limit [Å]	1.900 *	1.900 *
Rmerge	0.089 *
Total number of observations	140232 *
Number of reflections	9775 *
Completeness [%]	81.1 *	47.9 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	7-10 (mg/ml)
2	1	drop	potassium phosphate	0.5 (M)
3	1	drop	ammonium sulfate	1.2 (M)
4	1	reservoir	ammonium sulfate	3.5 (M)