5FCM
CrBld10-N 1-70
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-07-03 |
| Detector | DECTRIS PILATUS 2M |
| Wavelength(s) | 2.06642 |
| Spacegroup name | I 41 2 2 |
| Unit cell lengths | 92.740, 92.740, 164.070 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.109 - 2.229 |
| R-factor | 0.2154 |
| Rwork | 0.214 |
| R-free | 0.23640 |
| Structure solution method | SAD |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.560 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | SHELXDE |
| Refinement software | PHENIX (dev_1965) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.110 | 2.309 |
| High resolution limit [Å] | 2.229 | 2.229 |
| Rmerge | 0.107 | 2.160 |
| Number of reflections | 17823 | |
| <I/σ(I)> | 50.27 | 1.11 |
| Completeness [%] | 100.0 | 97 |
| Redundancy | 103.5 | 14.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M phosphate citrate, 5% 2-propanol, 0.2 M lithium sulfate |
