5FC1
Murine SMPDL3A in complex with sulfate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-09-03 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.97949 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 123.650, 131.870, 80.060 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.933 - 1.389 |
R-factor | 0.1313 |
Rwork | 0.130 |
R-free | 0.16070 |
RMSD bond length | 0.019 |
RMSD bond angle | 1.583 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.933 |
High resolution limit [Å] | 1.389 |
Number of reflections | 124089 |
<I/σ(I)> | 23.5 |
Completeness [%] | 94.7 |
Redundancy | 12.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293 | 0.2 M (NH4)2SO4, 0.1 M sodium acetate pH 4.6, 25% PEG 4000 |