5FC1

Murine SMPDL3A in complex with sulfate

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	100
Detector technology	CCD
Collection date	2013-09-03
Detector	RAYONIX MX-300
Wavelength(s)	0.97949
Spacegroup name	C 2 2 21
Unit cell lengths	123.650, 131.870, 80.060
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.933 - 1.389
R-factor	0.1313
Rwork	0.130
R-free	0.16070
RMSD bond length	0.019
RMSD bond angle	1.583
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	48.933
High resolution limit [Å]	1.389
Number of reflections	124089
<I/σ(I)>	23.5
Completeness [%]	94.7
Redundancy	12.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.6	293	0.2 M (NH4)2SO4, 0.1 M sodium acetate pH 4.6, 25% PEG 4000