5FA7
CTX-M-15 in complex with FPI-1523
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-07-15 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 1.00 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 62.730, 60.270, 76.010 |
Unit cell angles | 90.00, 112.78, 90.00 |
Refinement procedure
Resolution | 33.400 - 1.670 |
R-factor | 0.1767 |
Rwork | 0.175 |
R-free | 0.20650 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.120 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.0) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 70.100 |
High resolution limit [Å] | 1.670 |
Number of reflections | 59836 |
<I/σ(I)> | 12.2 |
Completeness [%] | 98.4 |
Redundancy | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298 | 0.2M ammonium sulfate, 0.1M MES pH6.5, 30% PEG5K monomethyl ether |