5F8F
Rv2258c-SFG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-10-04 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.9793 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 108.958, 141.118, 96.970 |
Unit cell angles | 90.00, 98.38, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.900 |
R-factor | 0.194 |
Rwork | 0.193 |
R-free | 0.22160 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.395 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0131) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.930 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 113690 | |
<I/σ(I)> | 28.8 | 2.8 |
Completeness [%] | 99.9 | |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 296 | sodium malonate, PEG 3350 |